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72 2,3,4-Tri- O -acetyl- α -d-glucuronic acid methyl ester and trichloroacetimidate (120.4 mg, 0.10 mmol) were added to the solution of 9 hydroxy corynantheidine (50 mg, 0.31 mmol) stirred in DCM (6 mL), over a molecular sieve, at rt under argon